Synthesis of Hierarchically Porous FAU/γ-Al 2 O 3 Composites with Different Morphologies Via Directing Agent Induced Method
CHINA PETROLEUM PROCESSING & PETROCHEMICAL TECHNOLOGY(2016)
Beijing Inst Technol
Abstract
Zeolite FAU composites with a macro/meso-microporous hierarchical structure were hydrothermally synthesized using macro-mesoporous γ-Al 2 O 3 monolith as the substrate by means of the liquid crystallization directing agent(LCDA) induced method. No template was needed throughout the synthesis processes. The structure and porosity of zeolite composites were analyzed by means of X-ray powder diffraction(XRD), scanning electron microscopy(SEM) and N 2 adsorption-desorption isotherms. The results showed that the supported zeolite composites with varied zeolitic crystalline phases and different morphologies can be obtained by adjusting the crystallization parameters, such as the crystallization temperature, the composition and the alkalinity of the precursor solution. The presence of LCDA was defined as a determinant for synthesizing the zeolite composites. The mechanisms for formation of the hierarchically porous FAU zeolite composites in the LCDA induced synthesis process were discussed. The resulting monolithic zeolite with a trimodal-porous hierarchical structure shows potential applicability where facile diffusion is required.
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Key words
monolithic FAU/gamma-Al2O3 composites,hierarchically porous,different morphologies,directing agent induced method
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