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Changes in the Microstructure and Mechanical Properties of Ti–6Al–4V Alloys Induced by Fe Ion Irradiation at a High He Generation Rate

Vacuum(2023)SCI 2区SCI 3区

Chinese Acad Sci

Cited 11|Views14
Abstract
As an attractive candidate structural material for nuclear applications, the irradiation resistance of high strength double-phase titanium alloys Ti-6Al-4V has received great attention. In this study, the damage dose dependence of defect evolution and hardening behavior at a high He generation rate (95 appm/dpa) for the Ti-6Al-4V alloys were investigated by TEM and nanoindentation. The Ti-6Al-4V specimen was pre-implanted with He ions with multi-energy at ambient temperature and subsequently irradiated with Fe ions at about 420 degrees C to obtain a He/ dpa plateau region (400-1000 nm) with average damage doses of 1.5, 7.5 and 37.5 dpa. TEM observations show that the bubble density showed a strong damage dose dependence. When irradiated to 37.5 dpa, the bubble exhibited a bimodal size distribution with the critical radius of approximately 1 nm. Meanwhile, the precipitate length showed an increasing trend with increasing depth, which is due to the effect of injected-Fe ions rather than the damage dose. In addition, no He dependence was observed for the loops and the precipitates. Nano -indentation results indicate that the irradiation hardening became more significant with the increase of damage dose. The contribution of irradiation-induced defects to the hardening was estimated by dispersed barrier -hardening (DBH) model.
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Key words
Ti-6Al-4V,Ion irradiation,Defect evolution,Irradiation hardening
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要点】:研究探讨了在高速氦生成率下,Fe离子辐照对Ti-6Al-4V合金微结构和力学性能的影响,发现辐照剂量对缺陷演化和硬化行为具有显著依赖性。

方法】:采用透射电镜(TEM)和纳米压痕技术,通过预植入He离子并在约420°C下用Fe离子辐照,研究不同辐照剂量下的微结构和力学性能变化。

实验】:在环境温度下对Ti-6Al-4V样品进行He离子预植入,随后在约420°C下用Fe离子辐照,达到平均辐照剂量为1.5、7.5和37.5 dpa的He/dpa平台区,通过TEM和纳米压痕分析得出辐照剂量对气泡密度、析出物长度及硬化行为的影响。