Experimental Investigation and Crystal Plasticity Modelling of Dynamic Recrystallisation in Dual-Phase High Entropy Alloy During Hot Deformation

Zixin Zhou,Yuanming Huo,Zhijun Wang,Eralp Demir, Anqi Jiang,Zhenrong Yan,Tao He

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING（2025）

Shanghai Univ Engn Sci | Northwestern Polytech Univ | Univ Oxford

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Abstract

During high-temperature processing, the Ni61Fe10Cr10Al17Mo2 high entropy alloy (HEA) often faces issues with uneven stress distribution and grain size, limiting its industrial applications. This study analyzes the dynamic recrystallisation (DRX) behavior and microstructural evolution of this alloy under high-temperature compression between 1100 degrees C and 1200 degrees C. High-temperature compression tests at strain rates of 0.2 and 0.7, combined with characterization techniques, reveal that DRX behavior significantly enhances with increasing temperature. The maximum grain size of 30.3 mu m was observed at 1200 degrees C while the maximum DRX fraction of 53.1 was observed at 1150 degrees C. In the initial stage of deformation, stress concentrates at the grain boundaries and interface boundary and then propagate to the deformation bands with temperature. The BCC phase undergoes continuous dynamic recrystallisation (CDRX), displaying significant differences from the DRX mechanism of the FCC phase, leading to asynchrony between the two phases during DRX. A crystal plasticity model incorporating dislocation density evolution successfully predicts stress softening and microstructural changes during high-temperature deformation. The initiation of DRX is highly temperature-sensitive, and the distinct mechanisms of the FCC and BCC phases jointly influence grain refinement and texture evolution. These findings provide theoretical support for the thermal processing of HEAs and for understanding their internal changes.

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Key words

High entropy alloy,Crystal plasticity,Dual phase,Dynamic recrystallisation,Dislocation density

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